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- W2935898279 abstract "In the present research, the process of the formation of the active components of Pd-Zn catalysts supported on carbonaceous material Sibunit prepared by the joint impregnation (Pd:Zn = 1) is studied. It was shown by means of TPR and EXAFS techniques that the interaction between palladium and zinc begins already at T > 200 °C. During the reduction in hydrogen at temperatures of 200–300 °C the surface of particles being formed is enriched with oxidized zinc. In the temperature range of 400–500 °C zinc is completely reduced, and the crystal lattice of a substitutional solid solution based on fcc lattice of palladium is restructured in tetragonal lattice of PdZn. However, an increase of the calcination temperature in H2 atmosphere (500 °C) significantly rises up the probability of partial destruction of bimetallic phase due to the partial migration of zinc atoms from the surface into the bulk of particles." @default.
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- W2935898279 date "2019-07-01" @default.
- W2935898279 modified "2023-10-18" @default.
- W2935898279 title "Study on the active phase formation of Pd-Zn/Sibunit catalysts during the thermal treatment in hydrogen" @default.
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- W2935898279 doi "https://doi.org/10.1016/j.apsusc.2019.03.215" @default.
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