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• W2937199098 abstract "A pyridine-mediated, one-pot synthesis of Zn0, Sn0, V0, and Mn0 nanoparticles is presented for the first time. Herein, pyridine is multifunctional, serving as a solvent, a reducing agent, and a surface-stabilizing agent. All metals were obtained as crystalline, spherical nanoparticles with very small sizes of 5.5 ± 0.6 nm (Zn0), 5.1 ± 0.7 nm (Sn0), 5.3 ± 0.6 nm (V0), and 6.9 ± 0.8 nm (Mn0). Simple metal chlorides (ZnCl2, SnCl2, VCl3, MnCl2) were used as the starting materials and heated in pyridine (autoclave, 210–300 °C). In addition to detailed particle characterization (high-resolution transmission electron microscopy, scanning transmission electron microscopy, Fourier-transformed infrared (FT-IR), X-ray powder diffraction, elemental analysis), the mechanism of reaction was explored (MS, NMR, FT-IR), indicating pyridine as the reducing agent that was oxidized to 2,2′-bipyridine. As a reliable and simple synthesis strategy, the novel pyridine-mediated approach can be highly relevant to obtain high-purity base-metal nanoparticles, and as a next step, to address widespread applications such as surface finishing of steel, catalysis, high-power batteries, or hydrogen storage." @default.
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• W2937199098 date "2019-04-19" @default.
• W2937199098 modified "2023-10-16" @default.
• W2937199098 title "One-Pot Synthesis of Reactive Base Metal Nanoparticles in Multifunctional Pyridine" @default.
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• W2937199098 doi "https://doi.org/10.1021/acsomega.9b00136" @default.
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