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• W2938301783 abstract "The electronic and structural properties of Au/ZnO under industrial and idealized methanol synthesis conditions have been investigated. This was achieved by kinetic measurements in combination with time-resolved operando infrared (DRIFTS) as well as in situ near-ambient pressure X-ray photoelectron spectroscopy (NAP-XPS) and X-ray absorption near-edge spectroscopy (XANES) measurements at the O K-edge together with high-resolution electron microscopy. The adsorption of CO during the reaction revealed the presence of negatively charged Au nanoparticles/Au sites during the initial phase of the reaction. Near-ambient-pressure XPS and XANES demonstrate the build-up of O vacancies during the reaction, which goes along with a substantial increase in the rate of methanol formation. The results are discussed in comparison with previous findings for Cu/ZnO and Au/ZnO catalysts." @default.
• W2938301783 created "2019-04-25" @default.
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• W2938301783 date "2019-06-18" @default.
• W2938301783 modified "2023-10-17" @default.
• W2938301783 title "Negative Charging of Au Nanoparticles during Methanol Synthesis from CO₂/H₂ on a Au/ZnO Catalyst: Insights from Operando IR and Near‐Ambient‐Pressure XPS and XAS Measurements" @default.
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• W2938301783 doi "https://doi.org/10.1002/anie.201900150" @default.
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• W2938301783 hasPublicationYear "2019" @default.
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