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- W2938850463 abstract "The synthesis of dinuclear copper(I) complexes of bibracchial tetraimine Schiff base macrocycles derived from the cyclocondensation of 2,5-diformylthiophene and the amines N,N-bis-(2-aminoethyl)-2-phenylethylamine, N,N-bis-(2-aminoethyl)-n-butylamine and N,N-bis-(2-aminoethyl)-t-butylamine is described. The structures of three such complexes are reported. The complex [Cu2L3(CH3CN)2](PF6)2·CH3CN crystallises in the monoclinic space group P21/c and has unit-cell dimensions a=15.897(4), b=13.329(4), c=21.999(5) Å, β=90.85(2)°, Z=4; the Cu–Cu separation is 5.201 Å. The complex [Cu2L4(CH3CN)2](PF6)2·0.64CH3CN crystallises in the monoclinic space group P21/n and has unit-cell dimensions a=17.243(5), b=11.451(6), c=26.534(8) Å, β=100.08(2)°, Z=4; the Cu–Cu separation is 5.386 Å. The complex [Cu2L6(CH3CN)2](PF6)2·CH3CN crystallises in the triclinic space group P1̄ and has unit-cell dimensions a=13.122(3), b=13.2116(3), c=13.718(3) Å, α=104.92(3)°, β=91.96(3)°, γ=96.19(3)°, Z=2; the Cu–Cu separation is 5.215 Å. In each complex there is a strongly bonded acetonitrile molecule coordinated to each copper atom. The reaction of [Cu2L3(CH3CN)2](PF6)2 with carbon monoxide is discussed." @default.
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- W2938850463 date "1998-01-01" @default.
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- W2938850463 title "Dinuclear copper(I) complexes of 24-membered bibracchial tetraimine Schiff base macrocycles derived from 2,5-diformylthiophene1Dedicated to Professor Ken Wade on the occasion of his 65th birthday in recognition of his outstanding contributions to inorganic chemistry.1" @default.
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- W2938850463 doi "https://doi.org/10.1016/s0022-328x(97)00041-7" @default.
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