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• W2939782783 abstract "13C-hyperpolarized carboxylates, such as pyruvate and acetate, are emerging molecular contrast agents for MRI visualization of various diseases, including cancer. Here we present a systematic study of 1H and 13C parahydrogen-induced polarization of acetate and pyruvate esters with ethyl, propyl and allyl alcoholic moieties. It was found that allyl pyruvate is the most efficiently hyperpolarized compound from those under study, yielding 21% and 5.4% polarization of 1H and 13C nuclei, respectively, in CD3OD solutions. Allyl pyruvate and ethyl acetate were also hyperpolarized in aqueous phase using homogeneous hydrogenation with parahydrogen over water-soluble rhodium catalyst. 13C polarization of 0.82% and 2.1% was obtained for allyl pyruvate and ethyl acetate, respectively. 13C-hyperpolarized methanolic and aqueous solutions of allyl pyruvate and ethyl acetate were employed for in vitro MRI visualization, demonstrating the prospects for translation of the presented approach to biomedical in vivo studies." @default.
• W2939782783 created "2019-04-25" @default.
• W2939782783 creator A5021984252 @default.
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• W2939782783 date "2019-04-19" @default.
• W2939782783 modified "2023-10-14" @default.
• W2939782783 title "Parahydrogen-Induced Polarization of 1-¹³C-Acetates and 1-¹³C-Pyruvates Using Sidearm Hydrogenation of Vinyl, Allyl, and Propargyl Esters" @default.
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• W2939782783 doi "https://doi.org/10.1021/acs.jpcc.9b02041" @default.
• W2939782783 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/6664436" @default.
• W2939782783 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/31363383" @default.
• W2939782783 hasPublicationYear "2019" @default.
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