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• W2940606946 abstract "The conversion of concentrated 5-hydroxymethylfurfural (HMF) or fructose to 2,5-furandicarboxylic acid (FDCA), a renewable alternative to petroleum-derived terephthalate acid, is highly desirable but challenging for FDCA production in an industrial scale. In this contribution, DMSO/H2O mixture was demonstrated as an effective medium for the production of FDCA from high concentration of HMF or fructose. For example, FDCA yield up to 93% was achieved at 10 wt% HMF concentration in DMSO/H2O over commercially available Ru/C (2 equiv. NaHCO3, 130 °C, 4 MPa O2 and 12 h). Furthermore, an overall FDCA yield of 65% was achieved from concentrated fructose (19 wt%) through a facile two-step process. Notably, it is so far the highest HMF or fructose concentration employed for FDCA formation. As compared to pure water or DMSO, DMSO/H2O mixed system is able to stabilize HMF in an alkaline environment, which allows the efficient oxidation of HMF at high concentrations." @default.
• W2940606946 created "2019-05-03" @default.
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• W2940606946 date "2019-09-01" @default.
• W2940606946 modified "2023-10-17" @default.
• W2940606946 title "Efficient synthesis of bio-monomer 2,5-furandicarboxylic acid from concentrated 5-hydroxymethylfurfural or fructose in DMSO/H2O mixed solvent" @default.
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• W2940606946 doi "https://doi.org/10.1016/j.jiec.2019.04.038" @default.
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