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- W2945164784 abstract "Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications." @default.
- W2945164784 created "2019-05-29" @default.
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- W2945164784 date "2019-08-01" @default.
- W2945164784 modified "2023-10-15" @default.
- W2945164784 title "Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) via facile one pot nitridation process" @default.
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- W2945164784 doi "https://doi.org/10.1016/j.jallcom.2019.05.234" @default.
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