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• W2945212110 abstract "Abstract The decomposition of sulfur trioxide to produce sulfur dioxide and oxygen using a catalytic membrane reactor is technology that promises to improve the economic viability of the thermochemical water‐splitting Iodine‐Sulfur (IS) process for large‐scale CO 2 ‐free hydrogen production. The chemical stability of membrane materials under SO 3 , however, is a significant challenge for this strategy. In this study, microporous membranes with a layered structure that consisted of a membrane support prepared from α‐Al 2 O 3 , an intermediate layer prepared from silica‐zirconia, and a top layer prepared from bis (triethoxysilyl)ethane‐derived organosilica sols, were examined for stability under SO 3 and for use in SO 3 /O 2 separation. An α‐Al 2 O 3 support that features SiO 2 –ZrO 2 intermediate layers with large pore sizes and a high Si/Zr molar ratio showed excellent resistance to SO 3 , which was confirmed by N 2 adsorption, Energy Dispersive X‐ray Spectroscopy (EDS), and Scanning Electron Microscopy (SEM). These membranes also demonstrated a negligible change in gas permeance before and after SO 3 exposure. Subsequently, in binary‐component gas separation at 550°C, microporous organosilica‐derived membranes achieved an O 2 /SO 3 selectivity of 10 (much higher than the Knudsen selectivity of 1.6) while maintaining a high O 2 permeance of 2.5 × 10 −8 mol m –2 s –1 Pa –1 ." @default.
• W2945212110 created "2019-05-29" @default.
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• W2945212110 date "2019-05-31" @default.
• W2945212110 modified "2023-10-16" @default.
• W2945212110 title "Evaluating the chemical stability of metal oxides in SO ₃ and applications of SiO ₂ ‐based membranes to O ₂ /SO ₃ separation" @default.
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• W2945212110 doi "https://doi.org/10.1111/jace.16594" @default.
• W2945212110 hasPublicationYear "2019" @default.
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