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• W2945244516 startingPage "1129" @default.
• W2945244516 abstract "The complexation study of cis -protected and bare palladium(II) components with a new tridentate ligand, i.e., pyridine-3,5-diylbis(methylene) dinicotinate ( L1 ) is the focus of this work. Complexation of cis -Pd(tmeda)(NO 3 ) 2 with L1 at a 1:1 or 3:2 ratio produced [Pd(tmeda)( L1 )](NO 3 ) 2 ( 1a ). The reaction mixture obtained at 3:2 ratio upon prolonged heating, produced a small amount of [Pd 3 (tmeda) 3 ( L1 ) 2 ](NO 3 ) 6 ( 2a ). Complexation of Pd(NO 3 ) 2 with L1 at a 1:2 or 3:4 ratios afforded [Pd( L1 ) 2 ](NO 3 ) 2 ( 3a ) and [(NO 3 ) 2 @Pd 3 ( L1 ) 4 ](NO 3 ) 4 ( 4a ), respectively. The encapsulated NO 3 – ions of 4a undergo anion exchange with halides (F – , Cl – and Br – but not with I – ) to form [(X) 2 @Pd 3 ( L1 ) 4 ](NO 3 ) 4 5a–7a . The coordination behaviour of ligand L1 and some dynamic properties of these complexes are compared with a set of known complexes prepared using the regioisomeric ligand bis(pyridin-3-ylmethyl)pyridine-3,5-dicarboxylate ( L2 ). Importantly, a ligand isomerism phenomenon is claimed by considering complexes prepared from L1 and L2 ." @default.
• W2945244516 created "2019-05-29" @default.
• W2945244516 creator A5014823155 @default.
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• W2945244516 date "2019-05-21" @default.
• W2945244516 modified "2023-09-27" @default.
• W2945244516 title "Design of a double-decker coordination cage revisited to make new cages and exemplify ligand isomerism" @default.
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• W2945244516 doi "https://doi.org/10.3762/bjoc.15.109" @default.
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