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- W2945383208 abstract "A rapid analytical method for determining 90Sr in urine samples (1-2 L) was developed to assess the internal exposure of workers in a radiological emergency. Strontium in a urine sample was rapidly separated by phosphate co-precipitation, followed by extraction chromatography, and the 90Sr activity was determined by triple quadrupole inductively coupled plasma mass spectrometry (ICP-MS/MS). Measurement in the MS/MS mode with an O2 reaction gas flow rate 1 mL min-1 showed no tailing of 88Sr at m/z = 90 up to 50 mg L-1 Sr. The interferences of Ge, Se and Zr at m/z = 90 were successfully removed by phosphate co-precipitation, followed by extraction chromatography with a tandem column of Pre-filter, TRU and Sr resin. This analytical method was validated by the results of the analyses of synthetic urine samples (1.2-1.6 L) containing a known amount of 90Sr along with 1 mg of each of Ge, Se, Sr and Zr. The turnaround time for Sr purification from the urine sample and the 90Sr measurement by ICP-MS/MS was about 10 h. The detection limit of 90Sr was approximately 1 Bq per urine sample, which was lower than 15 Bq per urine after a day of intake giving 5 mSv of unplanned exposure of worker limited by Nuclear Regulation Authority of Japan." @default.
- W2945383208 created "2019-05-29" @default.
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- W2945383208 date "2019-08-01" @default.
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- W2945383208 title "Rapid analytical method of 90Sr in urine sample: Rapid separation of Sr by phosphate co-precipitation and extraction chromatography, followed by determination by triple quadrupole inductively coupled plasma mass spectrometry (ICP-MS/MS)" @default.
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- W2945383208 doi "https://doi.org/10.1016/j.apradiso.2019.05.026" @default.
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