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• W2945918020 abstract "Hymexazol is an efficient and low-toxicity soil fungicide. In this work, a fully continuous flow process for the synthesis of hymexazol has been developed. This process begins with combining ethyl acetoacetate and hydroxylamine hydrochloride to form a hydroxamic acid intermediate. The reaction solution is then quenched with concentrated hydrochloric acid to obtain the final product, hymexazol. Under the optimized process conditions, the total yield of the target product reached 86%. In addition, production was successfully scaled-up to a kilogram scale. The continuous flow method not only greatly decreases the reaction time but also significantly inhibits the side reactions." @default.
• W2945918020 created "2019-05-29" @default.
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• W2945918020 date "2019-05-15" @default.
• W2945918020 modified "2023-10-16" @default.
• W2945918020 title "A Continuous Flow Process for the Synthesis of Hymexazol" @default.
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• W2945918020 doi "https://doi.org/10.1021/acs.oprd.9b00047" @default.
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