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- W2945972384 abstract "Abstract Described is a tetrabutylammonium fluoride‐mediated hydroxyalkylation reaction of phenols with cyclic carbonates. This operationally simple method enables the synthesis of a variety of aryl β‐hydroxyethyl ethers in good to excellent yields with a very small amount of catalyst loading (0.1–1 mol%). Of particular note is the efficient conversion of aromatic diols and phloroglucinol to the corresponding bis‐ and tris‐hydroxyethylated products. To further showcase the versatility of this protocol, guaifenesin was prepared with a single step by the condensation of guaiacol and glycerol carbonate. We also developed a flow ethoxylation process permitting the continuous synthesis of multiflorol. magnified image" @default.
- W2945972384 created "2019-05-29" @default.
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- W2945972384 date "2019-07-01" @default.
- W2945972384 modified "2023-10-14" @default.
- W2945972384 title "Revisiting Hydroxyalkylation of Phenols with Cyclic Carbonates" @default.
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- W2945972384 doi "https://doi.org/10.1002/adsc.201900287" @default.
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