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- W2946692034 abstract "The design and synthesis of 3 d –4 f heterometallic coordination polymers have attracted much interest due to the intriguing diversity of their architectures and topologies. Pyridine-2,6-dicarboxylic acid (H 2 pydc) has a versatile coordination mode and has been used to construct multinuclear and heterometallic compounds. Two isostructural centrosymmetric 3 d –4 f coordination compounds constructed from pyridine-2,6-dicarboxylic acid and 4,4′-bipyridine (bpy), namely 4,4′-bipyridine-1,1′-diium diaquabis(μ 2 -pyridine-2,6-dicarboxylato)tetrakis(pyridine-2,6-dicarboxylato)bis[4-(pyridin-4-yl)pyridinium]cobalt(II)dieuropium(III) octahydrate, (C 10 H 10 N 2 )[CoEu 2 (C 10 H 9 N 2 ) 2 (C 7 H 3 NO 4 ) 6 (H 2 O) 2 ]·8H 2 O, (I), and 4,4′-bipyridine-1,1′-diium diaquabis(μ 2 -pyridine-2,6-dicarboxylato)tetrakis(pyridine-2,6-dicarboxylato)bis[4-(pyridin-4-yl)pyridinium]cobalt(II)diterbium(III) octahydrate, (C 10 H 10 N 2 )[CoTb 2 (C 10 H 9 N 2 ) 2 (C 7 H 3 NO 4 ) 6 (H 2 O) 2 ]·8H 2 O, (II), were synthesized under hydrothermal conditions and characterized by IR and fluorescence spectroscopy, thermogravimetric analysis and powder X-ray diffraction. Both compounds crystallize in the triclinic space group P overline{1}. The Eu III and Tb III cations adopt nine-coordinated distorted tricapped trigonal–prismatic geometries bridged by three pydc 2− ligands. The Co II cation has a six-coordination environment formed by two pydc 2− ligands, two bpy ligands and two coordinated water molecules. Adjacent molecules are connected by π–π stacking interactions to form a one-dimensional chain, which is further extended into a three-dimensional supramolecular network by multipoint hydrogen bonds." @default.
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- W2946692034 date "2019-05-20" @default.
- W2946692034 modified "2023-10-16" @default.
- W2946692034 title "Synthesis and characterization of two isostructural 3d–4f coordination compounds based on pyridine-2,6-dicarboxylic acid and 4,4′-bipyridine" @default.
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- W2946692034 doi "https://doi.org/10.1107/s2053229619006004" @default.
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