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• W2947127116 abstract "Here, we report the crystal structures and properties of Rb xNbSe2, with 0 ≤ x ≤ 0.5. With Rb intercalation, Rb xNbSe2 evolves from 2H (Phase I) for 0 ≤ x ≤ 0.025, to 6R (Phase II) for x ∼ 0.2 with space group R3 m (no. 166), and finally to 2H (Phase IV) for 0.375 ≤ x ≤ 0.5 with space group P63/ mmc (no. 194). In addition, Phase II is found to transform to a rare 6H structure (Phase III) with space group P63/ mmc (no. 194) by annealing at a relatively low temperature. We show the first 6H phase in the intercalated transition-metal dichalcogenides (TMDs) family obtained through a solid-state reaction. Moreover, both 6R and 6H phases are new polymorphs in the NbSe2 system. For the range 0.2 ≤ x ≤ 0.5 in Rb xNbSe2, we show metallic electronic transport behavior and a paramagnetic feature. The lack of superconductivity (SC) down to 2 K is most probably due to the decrease of hole carrier density with increasing Rb content. Through careful analysis of the structural data, we were able to assemble a phase diagram covering the range of 0 ≤ x ≤ 0.5 in Rb xNbSe2." @default.
• W2947127116 created "2019-06-07" @default.
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• W2947127116 date "2019-05-22" @default.
• W2947127116 modified "2023-10-18" @default.
• W2947127116 title "Effects of Rb Intercalation on NbSe₂: Phase Formation, Structure, and Physical Properties" @default.
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• W2947127116 doi "https://doi.org/10.1021/acs.inorgchem.9b00862" @default.
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• W2947127116 hasPublicationYear "2019" @default.
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