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- W2948797664 abstract "The present study reports the unbiased chemical etching of micron-sized ZSM-5 crystals with an NH4F solution, resulting in house-of-cards-like single crystals containing large rectangular cavities surrounded by thin (15–30 nm), flat, and highly crystalline walls. The formation of such house-of-cards-like architecture is a result of the preferential extraction of misoriented nanocrystalline domains followed by the uniform dissolution of the remaining part of the crystal. The characteristic features of NH4F-treated zeolites are the retention of framework composition (Si/Al) and Brønsted acidity, high crystallinity, a moderate increase in the external surface area, and increased accessibility to their active sites. Such a combination produces zeolite catalysts with superior performances (activity, stability, and coke resistance) in the ethanol-to-hydrocarbon conversion. The physicochemical properties of this newly engineered zeolite are compared to those of a hierarchical zeolite obtained by caustic leaching and zeolite nanosheets synthesized with a bifunctional template, a diquaternary ammonium-type surfactant." @default.
- W2948797664 created "2019-06-14" @default.
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- W2948797664 date "2019-06-09" @default.
- W2948797664 modified "2023-10-17" @default.
- W2948797664 title "Preparation of Single-Crystal “House-of-Cards”-like ZSM-5 and Their Performance in Ethanol-to-Hydrocarbon Conversion" @default.
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- W2948797664 doi "https://doi.org/10.1021/acs.chemmater.8b04970" @default.
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