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- W2949062843 abstract "The thia-analog of ambrettolide, 1,8-oxathiacyclohexadecan-2-one (3), was synthesized from ℇ-caprolactone (4). Cleavage of 4 with trimethylsilyl iodide in the presence of ethanol provided iodoester 5, that was converted to the thioether 6 by treatment with tetramethylthiourea and the monoalkoxide of 1,8-octanediol. Collaud cyclization furnished the target compound 3 that contrary to thiocyclopentadecanolides 7, 8 and 9 possesses an intense musk odor." @default.
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- W2949062843 date "1997-05-01" @default.
- W2949062843 modified "2023-09-24" @default.
- W2949062843 title "The Thia-Analog of Ambrettolide. Synthesis and Odor of 1,8-Oxathiacyclohexadecan-2-one" @default.
- W2949062843 doi "https://doi.org/10.1055/s-1997-3223" @default.
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