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- W2949085773 abstract "Abstract To confirm the potential usefulness of amino acid residues as protecting groups for sugar hydroxyls, methyl 2,3-di-O-glycyl-α-D-glucopyranoside (5) and methyl 4,6-di-O-glycyl-2,3-di-O-methyl-α-D-gluco-pyranoside (7) were synthesized as reference compounds. Conditions were then established for the removal of these aminoacyl groups from the sugar molecules. The reference compounds were easily prepared by condensation of methyl α-D-glucopyranoside derivatives with N-protected glycine in the presence of dicyclohexyl-carbodiimide (DCC). The aminoacyl groups were removed by alkaline treatment, as were conventional acyl groups and also with ease by enzymatic hydrolysis using Pronase E. Conventional ester and ether protecting groups are not removed by such enzymatic treatment. Removal of aminoacyl group from sugar moieties on a practical scale is also described." @default.
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- W2949085773 date "1984-11-13" @default.
- W2949085773 modified "2023-09-27" @default.
- W2949085773 title "ChemInform Abstract: SYNTHESES OF METHYL 2,3-DI-O-GLYCYL-α-D-GLUCOPYRANOSIDE AND 4,6-DI-O-GLYCYL-2,3-DI-O-METHYL-α-D-GLUCOPYRANOSIDE, AND REMOVAL OF AMINOACYL GROUPS FROM SUGAR MOIETIES" @default.
- W2949085773 cites W2087422793 @default.
- W2949085773 doi "https://doi.org/10.1002/chin.198446344" @default.
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