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- W2949094862 abstract "Titanium superoxide efficiently catalysed the oxidative esterification of aldehydes with alkylarenes or alcohols, under truly heterogeneous conditions, to afford the corresponding benzyl and alkyl esters in excellent yields. Mechanistic studies have established that this one pot direct oxidative esterification process proceeds through a radical pathway, proven by a FTIR spectral study of a titanium superoxide-aldehyde complex as well as spin trapping experiments with TEMPO. The intramolecular version of this protocol has been successfully demonstrated in the concise synthesis of 3-butylphthalide, an anti-convulsant drug." @default.
- W2949094862 created "2019-06-27" @default.
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- W2949094862 date "2016-02-01" @default.
- W2949094862 modified "2023-09-27" @default.
- W2949094862 title "ChemInform Abstract: Titanium Superoxide - A Stable Recyclable Heterogeneous Catalyst for Oxidative Esterification of Aldehydes with Alkylarenes or Alcohols Using TBHP as an Oxidant." @default.
- W2949094862 cites W1736564100 @default.
- W2949094862 doi "https://doi.org/10.1002/chin.201610082" @default.
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