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- W2949152912 abstract "A new method for the preparation of α-fluorovinyl thioethers is reported which involves the hydrofluorination of alkynyl sulfides with 3HF·Et3N, a process that requires Lewis acid activation using BF3·Et2O and TiF4. The method gives access to a range of α-fluorovinyl thioethers, some in high stereoselectivity with the Z-isomer predominating over the E-isomer. The α-fluorovinyl thioether motif has prospects as a steric and electronic mimetic of thioester enols and enolates, important intermediates in enzymatic C–C bond forming reactions. The method opens access to appropriate analogues for investigations in this direction." @default.
- W2949152912 created "2019-06-27" @default.
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- W2949152912 date "2016-01-02" @default.
- W2949152912 modified "2023-09-27" @default.
- W2949152912 title "ChemInform Abstract: Lewis Acid-Promoted Hydrofluorination of Alkynyl Sulfides to Generate α-Fluorovinyl Thioethers." @default.
- W2949152912 cites W1936035029 @default.
- W2949152912 doi "https://doi.org/10.1002/chin.201602083" @default.
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