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- W2949176831 endingPage "1989" @default.
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- W2949176831 abstract "The reaction of α,β-unsaturated CF3-containing ketones R1R2CCHCOCF3 1−4 with ammonium hydrosulfide was investigated. The structure of the enones was shown to influence the reaction path, and the corresponding six-membered sulfur heterocycles bearing trifluoromethyl groups, 5−8, or mercaptan, 9, were obtained. The reaction of 3-adamantylidene-1,1,1-trifluoropropan-2-one, 3, results in the corresponding four-membered heterocycle 8, which has a stable 2-thietanol fragment. The oxidation of sulfides 5−8 by hydrogen peroxide yields sulfones 10−12 or 1,3-sultine 13 (in the case of 8). Product stereochemistry and reaction mechanism are discussed." @default.
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- W2949176831 date "1996-01-01" @default.
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- W2949176831 title "Synthesis of CF<sub>3</sub>-Containing Sulfur Heterocycles. The First Stable 2-Thietanol Derivative" @default.
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- W2949176831 doi "https://doi.org/10.1021/jo951351c" @default.
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