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- W2949209510 abstract "An all-cis-functionalized cyclopropane template to connect the three peptide chains in a collagen model is designed. Stereoselective synthesis of cyclopropane-assembled collagen-model 2b with the minimum unit of Gly-Pro-Pro is based on a novel 1-seleno-2-silylethene [2 + 1] cycloaddition strategy. Reaction of the 1-seleno-2-silylethene 4 with triester-substituted olefin 5 in the presence of ZnI2 gives [2 + 1] cycloadduct 6 stereoselectively. Cyclopropane 6 is selectively transformed into triol 10 in four steps. The reaction of 10 and three equivalents of N-Boc-Pro-Pro-Gly-OH in the presence of WSC–DMAP and subsequent deprotection with TFA gives 2b." @default.
- W2949209510 created "2019-06-27" @default.
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- W2949209510 date "2010-05-23" @default.
- W2949209510 modified "2023-09-26" @default.
- W2949209510 title "ChemInform Abstract: Synthesis of Novel all-cis-functionalized Cyclopropane Template-Assembled Collagen Models." @default.
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- W2949209510 doi "https://doi.org/10.1002/chin.200149170" @default.
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