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- W2949228811 abstract "The structure of gold cyanide, AuCN, has been determined at 10 and 300 K using total neutron diffraction. The structure consists of infinite −Au−(CN)−Au−(CN)−Au−(CN)− linear chains, hexagonally packed, with the gold atoms in sheets. The Au−C and Au−N bond lengths are found to be identical, with dAu-C/N = 1.9703(5) Å at 300 K. This work supersedes a previous study, by others, which used Rietveld analysis of neutron Bragg diffraction in isolation, and found these bonds to have significantly different lengths (Δd = 0.24 Å) at 300 K. The total correlation function, T(r), at 10 and 300 K, has been modeled using information derived from total diffraction. The broadening of inter- and intrachain correlations differs markedly due to random displacements of the chains in the direction of the chain axes. This is a consequence of the relatively weak bonding between the chains. An explanation for the negative thermal expansion in the c-direction, which occurs between 10 and 300 K, is presented." @default.
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- W2949228811 date "2003-06-25" @default.
- W2949228811 modified "2023-10-12" @default.
- W2949228811 title "Structure of AuCN Determined from Total Neutron Diffraction" @default.
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- W2949228811 doi "https://doi.org/10.1021/ic0342043" @default.
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