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• W2949272039 endingPage "185" @default.
• W2949272039 startingPage "181" @default.
• W2949272039 abstract "A three dimensional lithium hydronium sulfate LiSO4·H3O [1], [space group Pna21 a=8.7785(12) Å, b=9.1297(12) Å, c=5.2799(7) Å, V=423.16(10) Å3] was synthesized via solvothermal methods using 1,5-naphthalenedisulfonic acid (1,5-NSA) as the source of sulfate ions. The structure of [1], determined by single crystal X-ray diffraction techniques, consists of corner sharing LiO4 and SO4 tetrahedra, forming an anionic 3-D open framework that is charge balanced by hydronium ions positioned within channels running along [001] and forming strong H-bonding with the framework oxygen atoms. Compound [1] undergoes two reversible phase transitions, involving reorientation of SO42− ions at pressures of approximately 2.5 and 5 GPa at room temperature, as evident from characteristic discontinuous frequency drops in the ν1 mode of the Raman spectra. Additionally, compound [1] forms dense β-lithium sulfate at 300 °C, as evident from temperature dependent powder XRD and combined reversible TGA-DSC experiments." @default.
• W2949272039 created "2019-06-27" @default.
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• W2949272039 date "2013-01-01" @default.
• W2949272039 modified "2023-09-26" @default.
• W2949272039 title "Synthesis, structural characterization and high pressure phase transitions of monolithium hydronium sulfate" @default.
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• W2949272039 doi "https://doi.org/10.1016/j.jssc.2012.08.061" @default.
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