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- W2949276396 abstract "A mild and selective transition metal free protocol for the conversion of propargylic alcohols to cyclic and acyclic α,β-unsaturated enones via the Rupe rearrangement is reported. The method utilizes the Brønsted acidic ionic liquid [BMIM-SO3H][OTf] as catalyst and [BMIM][PF6] as solvent and offers the potential for recycling and reuse of the IL solvent. The feasibility to synthesize bicyclic fused cyclopentenone derivatives via a Rupe → Aldol → Nazarov sequence utilizing this protocol has also been demonstrated." @default.
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- W2949276396 date "2013-11-01" @default.
- W2949276396 modified "2023-10-07" @default.
- W2949276396 title "Mild conversion of propargylic alcohols to α,β-unsaturated enones in ionic liquids (ILs); a new ‘metal free’ life for the Rupe rearrangement" @default.
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- W2949276396 doi "https://doi.org/10.1016/j.tetlet.2013.09.028" @default.
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