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- W2949284310 abstract "Sulfur-bridged [1·n](2,5)thiophenophanes (n = 4—6) were prepared by cyclization of dibromo derivatives of the corresponding linear oligo(thio-2,5-thienylenes) (1) on reactions with Na2S. The best results were obtained by heating 1 and Na2S in the presence of Cs2CO3 in NMP (24% yield for n = 4, 16% for n = 5, and 10% for n = 6). The reactions gave less satisfactory results either in the presence of CuI (Cu2O) or in the absence of these additives. The results of the X-ray structural analyses of these three compounds are also reported." @default.
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- W2949284310 date "1998-11-01" @default.
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- W2949284310 title "Synthesis and Structure of Sulfur-Bridged [1<sub>·<i>n</i></sub>](2,5)Thiophenophanes (<i>n</i>= 4—6)" @default.
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- W2949284310 doi "https://doi.org/10.1246/bcsj.71.2695" @default.
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