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- W2949328319 abstract "Using ammonium iodide as a catalyst and m-chloroperbenzoic acid as the oxidant, a novel and efficient procedure has been developed for phosphoryloxylactonisation of alkenoic acids in CH 3 CN at room temperature, which provides the corresponding phosphoryloxylactones in good yields. In this protocol, it is proposed that ammonium iodide catalyst is first oxidised to hypoiodous acid, which reacts with the alkenoic acid to afford the corresponding iodolactone. Then, the iodolactone is further transformed into a hypervalent iodine intermediate by continuing oxidation, and finally the in situ generated active iodine species reacts with a diaryl phosphate to furnish the phosphoryloxylactone end product." @default.
- W2949328319 created "2019-06-27" @default.
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- W2949328319 date "2014-10-01" @default.
- W2949328319 modified "2023-09-25" @default.
- W2949328319 title "Novel Phosphoryloxylactonisation of Pentenoic Acids Mediated by Ammonium Iodide" @default.
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- W2949328319 doi "https://doi.org/10.3184/174751914x14117493538131" @default.
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