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- W2949337618 abstract "Peroxofluoro complexes of the transition metals, viz. V, Nb, Ta, Mo and W, have been synthesized electrochemically using the sacrificial metal anodes in the presence of hydrogen peroxide (15%) and hydrofluoric acid (10%). These complexes have also been prepared by the dissolution of the metal powders in a mixture of hydrogen peroxide and hydrofluoric acid. While the monoperoxo complexes are formed at lower pH, higher pH is conducive to the formation of diperoxo complexes. The compounds have been characterized by elemental analysis and vibrational spectral studies. K2[MoO(O2)F4]·H2O and K2[WO(O2)F4]·H2O can oxidize triphenylphosphine to triphenylphosphine oxide in high yield." @default.
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- W2949337618 date "1993-03-01" @default.
- W2949337618 modified "2023-10-18" @default.
- W2949337618 title "First electrosynthesis of transition metal peroxofluoro complexes. Synthesis, characterization and reactivity of some peroxofluoro complexes" @default.
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- W2949337618 doi "https://doi.org/10.1016/s0277-5387(00)84986-4" @default.
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