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- W2949480003 abstract "Abstract The structure of a Ag 3 Pb 4 Bi 11 Se 22 microcrystal was determined using microfocussed synchrotron radiation. Several crystals from an inhomogeneous sample were characterized by transmission electron microscopy, which revealed the unit‐cell dimensions and the quarternary composition. A crystallite that was pre‐characterized this way was used for the microfocus experiment. The structure of Ag 3 Pb 4 Bi 11 Se 22 [space group C 2/ m , a = 13.853(3) Å, b = 4.2108(8) Å, c = 19.721(4) Å, β = 104.57(3)°, Z = 1, R 1 (all) = 0.032] is similar to that of the mineral dantopaite, which belongs to the pavonite‐type family. Slabs that correspond to sections of the NaCl structure type are interconnected by ribbon‐like elements from the GeS (SnS) structure type." @default.
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- W2949480003 date "2015-01-28" @default.
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- W2949480003 title "Crystal Structure Determination of Ag<sub>3</sub>Pb<sub>4</sub>Bi<sub>11</sub>Se<sub>22</sub>by Microfocussed Synchrotron Radiation" @default.
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- W2949480003 doi "https://doi.org/10.1002/zaac.201400559" @default.
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