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- W2949597052 abstract "We report an improved procedure using solid-supported triphenylphosphine for the concise synthesis of biologically relevant 2-phenylbenzothiazoles featuring a variety of substituents on both the benzothiazole and phenyl rings. Substituted 2-phenylbenzothiazoles were synthesized by heating equimolar quantities of 2-aminothiophenol disulfides with benzaldehydes and p-toluenesulfonic acid in the presence of polymer-supported triphenylphosphine in dimethylformamide/toluene. Appealing features of this new method include simple isolation of product (removal of phosphine oxide by-product by filtration), avoidance of column chromatography, and good yields of substituted 2-phenylbenzothiazole products.Supplemental materials are available for this article. Go to the publisher's online edition of Synthetic Communications® to view the free supplemental file." @default.
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- W2949597052 date "2013-12-12" @default.
- W2949597052 modified "2023-09-27" @default.
- W2949597052 title "ChemInform Abstract: Convenient Synthesis of Substituted 2-Phenylbenzothiazoles Using Solid-Supported Triphenylphosphine." @default.
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- W2949597052 doi "https://doi.org/10.1002/chin.201401146" @default.
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