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- W2949646972 abstract "Abstract Pb 2 As x P 14– x was synthesized by reacting the pnicogens in a lead melt in sealed silica ampoules. A mixture of hydrogen peroxide and glacial acetic acid removed lead from the final product. Pb 2 As x P 14– x represents the first lead arsenide phosphide adopting a new structure type. Systematic substitution of phosphorus by arsenic leads to the formation of Pb 2 As x P 14– x with x ~ 3.7, a compound with a two-dimensional arrangement of polypnictide layers, coordinated by Pb 2+ cations. Pb 2 As x P 14– x is structurally related to PbP 7 where a three-dimensional polyphosphide network is realized instead. The structure of Pb 2 As 3.7(1) P 10.3(1) was determined from single crystal X-ray diffraction data: space group P 2 1 2 1 2 1 (no. 19), a = 10.060(1), b = 10.500(1), c = 13.711(2) Å, and V = 1448.3(4) Å 3 . The structure is discussed relative to PbP 7 focusing on the differences in the polyanionic substructures of the two polypnictides." @default.
- W2949646972 created "2019-06-27" @default.
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- W2949646972 date "2016-05-01" @default.
- W2949646972 modified "2023-09-26" @default.
- W2949646972 title "Synthesis and structure determinantion of the first lead arsenide phosphide Pb2AsxP14–x (x ~ 3.7)" @default.
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- W2949646972 doi "https://doi.org/10.1515/znb-2016-0048" @default.
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