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- W2949652016 abstract "A sensitive technique for determination of germanium was investigated by atomic absorption spectrometry following volatile hydride generation. Of the three types of hydride generator and atomizer systems tested, direct transfer of the generated hydride into nitrogen-hydrogen flame for atomization was found to be suitable. The sensitivity was enhanced more than 40–60% in phosphoric acid medium as compared to hydrochloric acid, malic acid, or tartaric acid media. Interference of nickel(II), gold(III), and cobalt(II) in hydrochloric acid medium was reduced by adding ethylenediaminetetraacetate as a masking reagent or replacing the acid medium by malic acid. Detection limit and relative standard deviation of ten determinations of 0.5 μg germanium(IV) in 20 ml of 0.20 M phosphoric acid were 7 ng (S/N=2) and 4.3%, respectively, with 3 ml of 8 w/v % sodium tetrahydroborate solution. The method was applied to the determination of germanium in standard rocks, concentrations of germanium in JB-1 and JG-1 being eval..." @default.
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- W2949652016 date "1982-01-19" @default.
- W2949652016 modified "2023-09-25" @default.
- W2949652016 title "ChemInform Abstract: DETERMINATION OF GERMANIUM BY ATOMIC ABSORPTION SPECTROMETRY FOLLOWING VOLATILE HYDRIDE GENERATION" @default.
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- W2949652016 doi "https://doi.org/10.1002/chin.198203320" @default.
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