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- W2949713034 abstract "Abstract Palladium catalyzed direct C–H arylation of 3-bromoisothiazole-5-carbonitrile with aryl/hetaryl iodides in the presence of AgF gave 13 4-aryl/hetaryl-3-bromoisothiazole-5-carbonitriles. The scope of this arylation was investigated and explanations for the limitations proposed. 3-Bromoisothiazole-5-carboxamide was isolated as a side-product, and its formation was attributed to Ag+-catalyzed hydration of the C-5 nitrile. The analogous phenylation of 3-chloroisothiazole-5-carbonitrile and 3-bromoisothiazole-4-carboxamide gave 3-chloro-4-phenylisothiazole-5-carbonitrile and 3-bromo-5-phenylisothiazole-4-carboxamide in 83 and 64% yields, respectively." @default.
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- W2949713034 date "2014-09-01" @default.
- W2949713034 modified "2023-10-14" @default.
- W2949713034 title "Silver mediated direct C–H arylation of 3-bromoisothiazole-5-carbonitrile" @default.
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- W2949713034 doi "https://doi.org/10.1016/j.tet.2014.07.064" @default.
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