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- W2949827280 abstract "Reaction of 3-ethyl-1-azabicyclo[1.1.0]butane (1a) with chloroform-potassium tert-butoxide afforded a ring-opened product, 1,1-dichloro-2-aza-4-ethylpenta-1,4-diene (4a), which was characterized via conversion to the corresponding N-substituted 5-chloro-1,2,3,4-tetrazole, Sa. Reaction of 3-phenyl-1-azabicyclo-[1.1.0]butane (1b) with “Seyferth's reagent” (PhHgCCl2Br) afforded 1,1-dichloro-2-aza-4-phenylpenta-1,4-diene (4b), which also was characterized via conversion to a tetrazole derivative, i.e., 5b. Finally, the reaction of 1b with dichlorocarbene generated under phase transfer conditions (chloroform-sodium hydroxide-TEBA) was studied. At short reaction times (0.5 hour), the major reaction product was 4b. However, at longer reaction times (20–30 hours), two secondary products, 8 and 9, were formed which resulted via subsequent dichlorocyclopropanation of 4b." @default.
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- W2949827280 date "2010-08-05" @default.
- W2949827280 modified "2023-10-05" @default.
- W2949827280 title "ChemInform Abstract: Ring-Opening Reactions of 3-Substituted 1-Azabicyclo(1.1.0)butane with Dichlorocarbene." @default.
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- W2949827280 doi "https://doi.org/10.1002/chin.199630065" @default.
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