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• W2949832767 abstract "Octahedral molybdenum and tungsten clusters face-capped by chalcogens M6Q8 (M = Mo, W; Q = S, Se, Te) have drawn extensive attention because of the well-known molybdenum-based Chevrel phases. Water-soluble cyanide complexes of these clusters can be prepared by cluster excision from the solid-state compound Mo6Se8 or by ligand exchange from W6S8(4-tert-butylpyridine)6. The [W6S8(CN)6]6- cluster anion can, in turn, be used as a building block to construct 3-D extended coordination networks with transition metal cations M2+ (M = Mn, Fe, Co, Zn) as linking units. The novel 3-D structures were determined by X-ray crystallography to be two-fold interpenetrating distorted cubic networks of [M(II)(H2O)4]3[W6S8(CN)6]·xH2O (x ≈ 23; M = Mn, Fe, Co) or a rutile-like network of K2[Zn(H2O)2]2[W6S8(CN)6]·26H2O, both bridged through W−CN−M−NC−W linkages. The properties of the new network structures are investigated and factors relevant to the construction of network structures containing W6S8 clusters are discussed." @default.
• W2949832767 created "2019-06-27" @default.
• W2949832767 creator A5037275754 @default.
• W2949832767 creator A5087754090 @default.
• W2949832767 date "2002-07-17" @default.
• W2949832767 modified "2023-10-16" @default.
• W2949832767 title "3-D Coordination Network Structures Constructed from [W₆S₈(CN)₆]⁶^- Anions" @default.
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• W2949832767 doi "https://doi.org/10.1021/cm020103b" @default.
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