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- W2949840992 abstract "Two practical procedures are described for the synthesis of the N-alkoxy analogues of 3,4,5-trihydroxypiperidine. The key feature of these methods is the intramolecular N-cyclization of hydroxylamine derivatives which are readily obtained from the reduction of the corresponding oximes. One method is to reductively hydroxyaminate an aldehyde group in the presence of a primary tosylated alcohol which is subsequently cyclized in situ upon neutralization. The intramolecular Mitsunobu coupling of a hydroxylamine with a primary alcohol proved useful for the preparation of compounds which contained the trans diol structure." @default.
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- W2949840992 date "1998-08-21" @default.
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- W2949840992 title "<i>N</i>-Alkoxy Analogues of 3,4,5-Trihydroxypiperidine" @default.
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- W2949840992 doi "https://doi.org/10.1021/jo971535m" @default.
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