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• W2949852059 startingPage "926" @default.
• W2949852059 abstract "Crystals of a hydrazinium-based copper(I) sulfide salt, N4H9Cu7S4 (1), have been isolated by an ambient temperature solution-based process. In contrast to previously reported hydrazinium salts of main-group metal chalcogenides, which consist of isolated metal chalcogenide anions, and ACu7S4 (A = NH4+, Rb+, Tl+, K+), which contains a more three-dimensional Cu7S4- framework with partial Cu-site occupancy, the structure of 1 [P21, a = 6.8621(4) Å, b = 7.9851(4) Å, c = 10.0983(5) Å, β = 99.360(1)°, Z = 2] is composed of extended two-dimensional Cu7S4- slabs with full Cu-site occupancy. The Cu7S4- slabs are separated by a mixture of hydrazinium and hydrazine moieties. Thermal decomposition of 1 into copper(I) sulfide proceeds at a significantly lower temperature than that observed for analogous hydrazinium salts of previously considered metal chalcogenides, completing the transition at temperatures as low as 120 °C. Solutions of 1 may be used in the solution deposition of a range of Cu-containing chalcogenide films." @default.
• W2949852059 created "2019-06-27" @default.
• W2949852059 creator A5024058183 @default.
• W2949852059 date "2007-01-12" @default.
• W2949852059 modified "2023-09-25" @default.
• W2949852059 title "N₄H₉Cu₇S₄: A Hydrazinium-Based Salt with a Layered Cu₇S₄^- Framework" @default.
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• W2949852059 doi "https://doi.org/10.1021/ic0621291" @default.
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