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• W2950086122 abstract "A novel, in-situ synthesis of dichlorotriphenylphosphorane (Ph3PCl2) is accomplished upon combining PPh3 and the easily prepared hypervalent iodine reagent iodobenzene dichloride (PhICl2). The phosphorane is selectively generated in the presence of carboxylic acid or alcohol residues to rapidly produce acyl chlorides and alkyl chlorides in high yields. Addition of EtOH, PhOH, BnOH, Et2NH or CH2N2 results in the direct synthesis of esters, amides and diazo ketones from carboxylic acids." @default.
• W2950086122 created "2019-06-27" @default.
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• W2950086122 date "2016-07-29" @default.
• W2950086122 modified "2023-10-07" @default.
• W2950086122 title "Iodobenzene Dichloride in the Esterification and Amidation of Carboxylic Acids: In-Situ Synthesis of Ph₃PCl₂" @default.
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• W2950086122 doi "https://doi.org/10.1002/ejoc.201600714" @default.
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