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- W2950230847 abstract "Some hexagonal mesoporous silicas were attempted to use as a promoter for fine organic synthesis. Ti-HMS, a Ti-loaded hexagonal mesoporous silica, which possesses Lewis acid sites due to Ti-atom, was found to accelerate deprotection of benzyl ethers under hydrogenolytic conditions with palladium catalyst. Such acid-sensitive functional groups as silyl ether and acetal moieties in the molecule were little affected by Ti-HMS. MCM-41, a hexagonal mesoporous silica, /MeOH heterogeneous system was found to remove selectively and easily triethylsilyl (TES) group of silyl ethers of several types in the presence of t-butyldimethylsilyl (TBS) groups. FSM-16, another hexagonal mesoporous silica, was found to catalyze oxidative photodecarboxylation of alpha-hydroxy carboxylic acid and phenyl acetic acid derivatives to afford the corresponding carbonyl compounds. Furthermore, FSM-16 proved to be reuseable by recalcination at 450 degrees C after the reaction. Efficiency of these reactions was investigated concerning the solvent effect and activities of the promoters including common zeolites and ion-exchange resins." @default.
- W2950230847 created "2019-06-27" @default.
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- W2950230847 date "2000-01-01" @default.
- W2950230847 modified "2023-09-27" @default.
- W2950230847 title "Synthetic Organic Reactions with Mesoporous Silicas" @default.
- W2950230847 doi "https://doi.org/10.1248/yakushi1947.120.11_1105" @default.
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