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- W2950264799 abstract "Abstract The use of chiral tripodal ligands in the assembly of non-centrosymmetric crystal lattice is illustrated with the triamide ligand tris[ N -( S )-(−)-(α)-methylbenzylcarbamoylmethyl]amine (H 3 1 S -mbz ). In the crystal phase, this tripodal ligand assembles into C 3 -symmetric chiral columns that are stabilized by hydrogen bonds and aryl–aryl interactions. Intercolumnar assembly is driven by the clustering of edge-to-face aryl and methyl-to-aryl interactions. Thrice deprotonation of H 3 1 S -mbz and binding of an Ni(II)–F moiety also produces a non-centrosymmetric lattice which is noteworthy for its six-fold symmetric open framework structure and the alignment of all the molecular Ni–F bonds in the lattice along the crystallographic c -axis. Crystal data: H 3 1 S -mbz crystallizes in the rhombohedral system, space group R 3 with cell dimensions a = b =22.352(5) A, c =4.882(1) A, α = β =90°, γ =120°, and Z =3; [NEt 4 ] 2 [Ni 1 S -mbz (F)] crystallizes in the hexagonal system, space group P 6 3 with cell dimensions a = b =12.0780(1) A, c =18.1231(1) A, α = β =90°, γ =120°, and Z =2." @default.
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- W2950264799 date "2010-06-18" @default.
- W2950264799 modified "2023-09-26" @default.
- W2950264799 title "ChemInform Abstract: The Use of C3-Symmetric Tripodal Ligands in Crystal Engineering" @default.
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- W2950264799 doi "https://doi.org/10.1002/chin.199903257" @default.
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