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- W2950302814 endingPage "51" @default.
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- W2950302814 abstract "A new synthetic strategy for one-pot synthesis of a fluorinated isopolyvanadate, (NMe4)4[V12O30F4(H2O)2]·9H2O, utilizing peroxidovanadate intermediates, and the stepwise characterization of the reaction mixture is reported herein. The characterization of the title compound was done by single-crystal X-ray diffraction and IR spectroscopy and the reactivity was monitored by 51V NMR spectroscopy to elucidate the hydrolysis pathway. The [V12O30F4(H2O)2]4 − anion consists of four VO5 units in the central layer and two groups of three VO5F units capped by one VO4F(H2O) unit in the outer layers of the anion. In the crystal structure, the anions form strong O–H⋯F hydrogen bonds running in the a axis direction." @default.
- W2950302814 created "2019-06-27" @default.
- W2950302814 creator A5025144005 @default.
- W2950302814 creator A5031694583 @default.
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- W2950302814 date "2014-11-01" @default.
- W2950302814 modified "2023-10-01" @default.
- W2950302814 title "[V12O30F4(H2O)2]4−: One-pot synthesis and characterization of a novel fluorinated dodecavanadate" @default.
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- W2950302814 doi "https://doi.org/10.1016/j.inoche.2014.09.017" @default.
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