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- W2950302871 abstract "Two new ternary uranium selenides, AU 2 Se 6 (A = K, Cs), were prepared using the reactive flux method. Single crystal X-ray diffraction was performed on single crystals. The compounds crystallize in the orthorhombic Immm space group, Z = 2. CsU 2 Se 6 has cell parameters of a = 4.046(2) A, b = 5.559(3) A, and c = 24.237(12) A. KU 2 Se 6 has cell parameters of a = 4.058(3) A, b = 5.556(4) A, and c = 21.710(17) A. The compounds are isostructural to the previously reported KTh 2 Se 6 . The two-dimensional layered structure is related to ZrSe 3 with the alkali metals residing in the interlayer space. The oxidation states of uranium and selenium were evaluated using X-ray photoelectron spectroscopy (XPS). Uranium was found to be tetravalent, while selenium was found to be in two oxidation states, one of which is -2. The other oxidation state is similar to that found in a polyselenide network. While this structure is known, our work examines how the structure changes through the transactinide series." @default.
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- W2950302871 date "2004-07-06" @default.
- W2950302871 modified "2023-09-27" @default.
- W2950302871 title "Synthesis and Characterization of AU2Se6 (A: K, Cs)." @default.
- W2950302871 cites W2084050344 @default.
- W2950302871 doi "https://doi.org/10.1002/chin.200427026" @default.
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