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- W2950339922 abstract "The effects of reaction temperature and pO2 were investigated on a series of (Ba,Ca,Nd)FeO3-δ perovskite systems in order to isolate phases containing ordered arrangements of the distinct vacancy and cation ordering patterns identified in less compositionally complex iron oxide systems. Initial synthesis in air at high temperature yields cubic perovskite phases (I) with average iron oxidation states higher than 3; selected area electron diffraction together with diffuse features observed in the synchrotron X-ray diffraction (SXRD) patterns of these materials show evidence of small domains of short-range cation and vacancy order. Annealing these materials in nitrogen or in a sealed tube in the presence of an NiO/Ni buffer yielded the Fe3+ phase Ca2Ba2Nd2Fe6O16 (II), closely related to Sr2LaFe3O8 but with partial cation order as well as anion order present—the larger Ba cations are largely present in the 12-coordinate site between the octahedral iron layers, and Ca is largely present in 10-coordinate sites ..." @default.
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- W2950339922 date "2008-09-16" @default.
- W2950339922 modified "2023-09-26" @default.
- W2950339922 title "ChemInform Abstract: Modular Construction of Oxide Structures-Compositional Control of Transition Metal Coordination Environments." @default.
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- W2950339922 doi "https://doi.org/10.1002/chin.200838028" @default.
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