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- W2950366012 abstract "Cotunnite-type zirconia was studied by angular-dispersive X-ray diffraction in a diamond anvil cell after laser heating and 18 and 26.7 GPa. The structure, space group Pnam, Z = 4, was refined in situ at several different pressures on decompression and at ambient using the Rietveld method. The nine polyhedral Zr-O distances range from 2.10 to 2.56 {angstrom} at ambient pressure, which represents both an increase in the average and the minimum Zr-O distance relative to the monoclinic and orthorhombic lower-pressure forms. In addition, data obtained on an unheated sample indicate that the irreversible transition to the cotunnite phase began above 25 GPa and 70% conversion was achieved by 48.5 GPa. The compressibility of cotunnite-type zirconia was found to be slightly anisotropic and a Birch-Murnaghan equation-of-state fit of the p-V data yielded a bulk modulus of 332(8) GPa with a first derivative of 2.3(4), which is in good agreement with the value predicted by previous ab initio calculations." @default.
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- W2950366012 date "2010-08-05" @default.
- W2950366012 modified "2023-09-27" @default.
- W2950366012 title "ChemInform Abstract: Crystal Structure and Equation of State of Cotunnite-Type Zirconia." @default.
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- W2950366012 doi "https://doi.org/10.1002/chin.199618001" @default.
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