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• W2950372912 abstract "Various chiral non-racemic β-ketosulfoxides, a class of compounds frequently used in asymmetric synthesis, were prepared in good yields by tert-butyl hydroperoxide oxidation of the corresponding sulfides in the presence of a complex between titanium and (S,S)-hydrobenzoin. The ee values of almost all of the purified products were >98%. As ascertained by X-ray analysis and/or by NMR spectroscopy, the use of the (S,S)-form of the ligand led to aryl β-ketosulfoxides with (RS)-configuration and to methyl phenacyl sulfoxide with the (SS)-configuration. Some of the aryl ketosulfoxides were subjected to reduction with DIBAL-H/ZnCl2 and the corresponding β-sulfinylalcohols with an (R,RS)-configuration produced." @default.
• W2950372912 created "2019-06-27" @default.
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• W2950372912 date "2006-01-01" @default.
• W2950372912 modified "2023-09-27" @default.
• W2950372912 title "The synthesis of chiral β-ketosulfoxides by enantioselective oxidation and their stereocontrolled reduction to β-hydroxysulfoxides" @default.
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• W2950372912 doi "https://doi.org/10.1016/j.tetasy.2005.12.004" @default.
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