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- W2950396003 abstract "The dimethylamino-substituted phosphaalkene 1 reacts with hexafluoroacetone (HFA) with addition at the PC bond to form the 1,5,2-dioxaphosphorinane 2. The structure of 2 was confirmed by an X-ray crystal structure analysis. The six-membered ring displays an envelope conformation with the phosphorus atom out of the plane, but the phosphorus is disordered over two sites. Reaction of P-trimethylsilyl-substituted phosphaalkenes with HFA proceeds with retention of the PC double bond and insertion of HFA into the PSi bond. Two isomeric products are obtained and are characterized by 1H-, 13C-, 19F-, and 31P-NMR spectroscopy, IR spectroscopy, mass spectrometry, and elemental analysis." @default.
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- W2950396003 date "1995-05-01" @default.
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- W2950396003 title "Reactions of Phosphaalkenes with Hexafluoroacetone" @default.
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- W2950396003 doi "https://doi.org/10.1002/cber.19951280511" @default.
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