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- W2950477576 abstract "Treatment of dialkyl 1,1-difluoromethylenephosphonates 1 with Lawesson's reagent cleanly produces the corresponding dialkyl 1,1-difluoromethylenephosphonothioates 2. The reaction can be extended to dialkyl 1,1-difluoromethylenephosphinates and to dialkyl 1,1-difluoromethylenephosphine oxides. The reversed transformation (i.e. converting dialkyl 1,1-difluoromethylenephosphonothioates into dialkyl 1,1-difluoromethylenephosphonates) is most conveniently achieved by using dioxirane 7 or perfluoro-cis-2-n-butyl-3-n-propyloxaziridine 8, and produces the desired phosphonates in high yield. The synthetic interest of these transformations is discussed." @default.
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- W2950477576 date "1996-07-01" @default.
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- W2950477576 title "Efficient interconversion of α,α-difluoromethylenephosphonates and α,α-difluoromethylenephosphonothioates" @default.
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- W2950477576 doi "https://doi.org/10.1016/0040-4039(96)00912-4" @default.
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