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- W2950501156 abstract "A series of 4 H-5,6,7,8-tetrahydrobenzo[ b]pyran derivatives has been synthesised in excellent yield in a single pot using trioctylmethylammonium chloride (Aliquat®336) as phase-transfer catalyst in water under microwave irradiation. This method provides a clean access to the desired products. The structures of the products were confirmed by IR, 1 H NMR, 13 C NMR in all cases and HRMS in several cases, and supported by single crystal X-ray diffraction analysis of 2-amino-4-(3-benzyloxy-4-methoxyphenyl)-3-cyano-7,7-dimethyl-5-oxo-4 H-5,6,7,8-tetrahydrobenzo[ b]pyran and 2-amino-3-cyano-4-(3-iodo-4-hydroxy-5-methoxyphenyl)-7,7-dimethyl-5-oxo-4 H-5,6,7,8-tetrahydrobenzo[ b] pyran." @default.
- W2950501156 created "2019-06-27" @default.
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- W2950501156 creator A5057535487 @default.
- W2950501156 date "2010-12-01" @default.
- W2950501156 modified "2023-10-11" @default.
- W2950501156 title "Synthesis of Tetrahydrobenzo[<i>b</i>]Pyran Derivatives Catalysed by Aliquat®336 in Water Under Microwave Irradiation" @default.
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- W2950501156 doi "https://doi.org/10.3184/030823410x12857507693346" @default.
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