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- W2950532823 abstract "Abstract The intermetallic compounds Mg 0.39(2) NiSn 1.61(2) and Mg 2.61(2) Ni 4 Sn 3.39(2) are prepared by the reaction of the elements in welded tantalum ampoules in a resistance furnace. The crystal structures of the compounds were investigated by single‐crystal X‐ray diffraction. Mg 0.39(2) NiSn 1.61(2) crystallizes in the PdSn 2 structure type with the space group I 4 1 / acd [ a = 6.1941(4) Å, c = 23.498(2) Å, wR 2 = 0.078 (all data), 303 F 2 values, 19 variable parameters]. The main building block in the crystal structure of Mg 0.39(2) NiSn 1.61(2) are Ni 2 @(Mg/Sn) 12 polyhedra, which consist of face‐sharing Ni‐centered square antiprisms. These polyhedra share vertices to form a three‐dimensional network of Mg and Sn atoms. The mixing of small amounts of magnesium in the binary Ni‐Sn phase stabilizes the non‐existing “NiSn 2 ” in the PdSn 2 structure type in form of NiSn 2– x Mg x with x = 0.39. Mg 2.61(2) Ni 4 Sn 3.39(2) crystallizes in an own structure type with space group P $bar{3}$ m 1 [ a = 4.3230(9) Å, c = 10.490(3) Å, wR 2 = 0.048 (all data), 216 F 2 values, 21 variable parameters]. The crystal structure of Mg 2.61(2) Ni 4 Sn 3.39(2) is described as an intermediate of a Heusler and a Half‐Heusler type structure what is demonstrated by group‐subgroup relationships." @default.
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- W2950532823 date "2015-02-01" @default.
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- W2950532823 title "Crystal Structure of Mg<sub>0.39(2)</sub>NiSn<sub>1.61(2)</sub> and Mg<sub>2.61(2)</sub>Ni<sub>4</sub>Sn<sub>3.39(2)</sub> Featuring Mg/Sn Atom Networks with Different Connections of Ni@(Mg/Sn)<sub>8</sub> Coordination Polyhedra" @default.
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- W2950532823 doi "https://doi.org/10.1002/zaac.201400546" @default.
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