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- W2950577586 abstract "Single crystals of several phases in the Na–V–(O)F and K–V–(O)F systems have been grown using a mild solvothermal route in water/ethylene glycol. At a temperature of 100 °C the V4+-containing oxyfluoride phases Na4V2O2F8 and K2VOF4 are prepared, exhibiting dimeric and chain-like vanadium oxyfluoride units, respectively. On raising the reaction temperature to 220 °C reduction to V3+ occurs, and three different two-dimensional sheet structures are crystallised, NaVF4, KVF4 and K5V3F14. Precise crystal structures are reported for the latter two, which represent members of the Dion–Jacobson and Chiolite families, respectively." @default.
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- W2950577586 date "2009-02-01" @default.
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- W2950577586 title "Crystallisation of some mixed Na/V and K/V fluorides by solvothermal methods" @default.
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- W2950577586 doi "https://doi.org/10.1016/j.solidstatesciences.2008.09.003" @default.
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