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• W2950586466 endingPage "7751" @default.
• W2950586466 startingPage "7747" @default.
• W2950586466 abstract "The two ternary uranium thiophosphate compounds were isolated from polychalcogenide flux reactions. UP2S9 crystallizes in the tetragonal space group P42/mcm with two formula units per unit cell, where a = 7.762(1) and c = 9.691(3) Å. UP2S7 crystallizes in the orthorhombic space group Fddd with 16 formula units per unit cell, here a = 8.919(3), b = 15.198(4), and c = 30.104(9) Å. Both compounds were characterized through single crystal X-ray, UV–vis–NIR, and Raman spectroscopy. The structures of the two compounds are formed from [US6]8– chains connected to each other by either the tridentate-chelating P2S94– in UP2S9 or the P2S74– in UP2S7 resulting in 3D frameworks. These two ligands have different geometries, but they exhibit similar coordination modes, comparable to the ethane-like P2S64–. The uranium cations in both compounds can be assigned an unambiguous oxidation state of +4. The two compounds are semiconductors with nearly identical band-gaps of 1.41 eV." @default.
• W2950586466 created "2019-06-27" @default.
• W2950586466 creator A5017039673 @default.
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• W2950586466 date "2013-06-17" @default.
• W2950586466 modified "2023-09-23" @default.
• W2950586466 title "Synthesis, Structure, and Spectroscopy of Two Ternary Uranium(IV) Thiophosphates: UP₂S₉ and UP₂S₇ Containing P₂S₉^2– and P₂S₇^2– Ligands" @default.
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• W2950586466 doi "https://doi.org/10.1021/ic400942r" @default.
• W2950586466 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23773125" @default.
• W2950586466 hasPublicationYear "2013" @default.
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